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CHEM GU4148 Synthetic Methods in Organic Chemistry I. 4.5 points.

Students will apply laboratory techniques learned in CHE350A to synthesize , purify and identify organic compounds including alcohols, aldehydes, aromatics, ketones, ethers, esters, amides and amines. The experiments will be done on a small scale approach or microscale. Contact hours for this laboratory course (45) are based on a 3:1 ratio, i.e. 3 Lab hours= 1 lecture hour equivalent.

The principles of organic chemistry. The structure and reactivity of organic molecules are examined from the standpoint of modern theories of chemistry. Topics include stereochemistry, reactions of organic molecules, mechanisms of organic reactions, syntheses and degradations of organic molecules, and spectroscopic techniques of structure determination. Although CHEM UN2443 and CHEM UN2444 are separate courses, students are expected to take both terms sequentially. Students must ensure they register for the recitation which corresponds to the lecture section. Please check the Directory of Classes for details.

Text: Introduction to Organic Laboratory Techniques: A Small Scale ..

Small Scale Synthesis: A Laboratory Text of Organic Chemistry

Organic Chemistry Laboratory II (Synthesis) ..

intraperitoneal IPCS International Programme on Chemical Safety JECFA Joint FAO/WHO Expert Committee on Food Additives LD50 median lethal dose LDH lactate dehydrogenase LDL low-density lipoprotein LOAEL lowest-observed-adverse-effect level MA 3,4-(dichloro)-5-hydroxy-2(5H)-furanone MBA monobromoacetic acid/monobromoacetate MCA monochloroacetic acid/monochloroacetate MNU methylnitrosourea MOR mortality odds ratio MRI magnetic resonance imaging MTBE methyl tert-butyl ether MX 3-chloro-4-(dichloromethyl)-5-hydroxy-2(5H)-furanone NADP nicotinamide adenine dinucleotide phosphate NOAEL no-observed-adverse-effect level NOEL no-observed-effect level NOM natural organic matter NTP National Toxicology Program (USA) 8-OH-dG 8-hydroxy-2-deoxyguanosine OR odds ratio PAS periodic acid/Schiff's reagent PBPK physiologically based pharmacokinetic model PFBHA O-(2,3,4,5,6-pentafluorobenzyl)-hydroxylamine p Ka log acid dissociation constant PPAR peroxisome proliferator activated receptor PPRE peroxisome proliferator responsive element RR relative risk SCE sister chromatid exchange SD standard deviation SDH sorbitol dehydrogenase SE standard error SGOT serum glutamate-oxaloacetate transaminase SGPT serum glutamate-pyruvate transaminase SMR standardized mortality ratio SSB single strand breaks TBA tribromoacetic acid/tribromoacetate TBARS thiobarbituric acid reactive substances TCA trichloroacetic acid/trichloroacetate TCAN trichloroacetonitrile TCPN trichloropropanone TDI tolerable daily intake TGF transforming growth factor THM trihalomethane TOC total organic carbon TOX total organic halogen TPA 12- O-tetradecanoylphorbol-13-acetate UDS unscheduled DNA synthesis UV ultraviolet UVA254 UV absorbance at 254 nm Vmax maximum rate of metabolism WHO World Health Organization 1.

Polymeric materials have long been ubiquitous items and played important roles in revolutionizing the way we live. Due to the advent of modern polymerization fabrication strategies, polymers are rapidly gaining interest for the development of next generation devices and medical treatment. This course will focus on the chemistry polymers and their use as nanostructured materials created by self-assembly and top-down fabrication techniques. Specifically, the class will be divided into two sections describing the uses of organic nanostructures on a) surfaces and b) as particles. Patterned surfaces will be described in terms of photo-, imprint-, and block copolymer lithography. The preparation of nanoparticles through polymer synthesis, dendrimers, and mechanical manipulation will be the second part.

Simple and Versatile Laboratory Scale CSTR for …

This is an introductory course to the field of inorganic nanomaterials chemistry. The course will cover the synthesis, the structural, electronic and magnetic characterization, and the physical properties of zero-, one- and two-dimensional inorganic nanomaterials. Particular emphasis will be devoted to the design of building blocks that can organize into functional assemblies and to the emergence of collective physical properties. The course will also explore the recent and developing electronic and optoelectronic applications of these materials.

Small Scale Synthesis: A Laboratory Text of Organic Chemistry by Murray Zanger. McGraw-Hill Education. Spiral-bound. Good. Ships with Tracking Number!

Presents multi-step synthesis and identification of unknown mixtures including chemical, physical and spectroscopic studies of aliphatic and aromatic alcohols, aldehydes, ketones, acids and other classes of organic compounds. Includes GC and IR. Students enrolled in the Honors Transfer Program may count this course towards the "Honors Scholar" designation with an Honors Contract.

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Martindale's Calculators On-Line Center: Chemistry …


DISINFECTANTS AND DISINFECTANT BY-PRODUCTS

Please note that you must complete before you register for . This lab introduces students to experimental design and trains students in the execution and evaluation of scientific data. The technique experiments in the first half of the course () teach students to develop and master the required experimental skills to perform the challenging synthesis experiments in the second semester. The learning outcomes for this lab are the knowledge and experimental skills associated with the most important synthetic routes widely used in industrial and research environments. Attendance at the first lab lecture and laboratory session is mandatory. Please note that is the second part of a full year organic chemistry laboratory course. Students must register for the lab lecture section () which corresponds to their lab section. Students must attend ONE lab lecture and ONE lab section every other week. Please contact your advisers for further information.

Chlorinated Paraffins (EHC 181, 1996) - INCHEM

Carbon-carbon bond-forming reactions; alkene synthesis; oxidation; reductions; function group interconversion; use of protecting groups; and organometallic reagents.

A Scalable Route for the Regio- and …

The principles of organic chemistry. The structure and reactivity of organic molecules are examined from the standpoint of modern theories of chemistry. Topics include stereochemistry, reactions of organic molecules, mechanisms of organic reactions, syntheses and degradations of organic molecules, and spectroscopic techniques of structure determination. Although CHEM UN2443 and CHEM UN2444 are separate courses, students are expected to take both terms sequentially. Students must ensure they register for the recitation which corresponds to the lecture section. Please check the Directory of Classes for details.

Hydrazine is a precursor to several pharmaceuticals and pesticides

This course is intended for graduate students and advanced undergraduate students. The main purpose of the course is to introduce students to modern synthetic chemistry via the selected series of topics (synthetic planning and the logic of organic assembly, classical and new reactions/methods and their use in complex target synthesis). Mechanistic underpinning of the discussed reaction processes will also be briefly discussed. For each module (see the content below), specific examples of syntheses of natural products and/or synthetic materials will be provided. In addition to lectures by Prof. Sames, students will select and present relevant papers in the class (the number of student symposia will depend on the final enrollment in this course). The basic knowledge of transition metal chemistry is recommended for the cross-coupling reactions (i.e., structure, electron counting, and elemental reaction types of transition metals).

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